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Spectrophotometric determination of bacitracin in bulk drug as dabsyl derivative in a range of visible light
2011
journal article
article
Journal
Acta Poloniae Pharmaceutica. Drug Research
Author
Krzek Jan
Piotrowska Joanna
Volume
68
Number
6
Pages
853-858
ISSN
0001-6837
eISSN
2353-5288
Keywords in English
bacitracin
dabsyl chloride
VIS spectrophotometry
Access date
2020-07-28
Remarks
Bibliogr. s. 858
Language
English
Journal language
English
Abstract in English
A fast spectrophotometric method has been developed for bacitracin identification and determination after condensation reaction with dabsyl chloride. In addition, determination of dye stability of sulfonamide derivative and identification of the molar ratio of reagents was done at various time-points. The developed method has a good linearity with very broad spectrum, correlation coefficient of r = 0.9972, good precision (RSD = 1.54 ± 0.11%), and recovery at three different levels of concentration was found between 98.33% and 103.47%. Usefulness of the method was demonstrated by positive results obtained during determination of bacitracin concentration in bulk drug.
Affiliation
Wydział Farmaceutyczny : Zakład Chemii NieorganicznejWydział Farmaceutyczny : Zakład Chemii Analitycznej
| dc.abstract.en | A fast spectrophotometric method has been developed for bacitracin identification and determination after condensation reaction with dabsyl chloride. In addition, determination of dye stability of sulfonamide derivative and identification of the molar ratio of reagents was done at various time-points. The developed method has a good linearity with very broad spectrum, correlation coefficient of r = 0.9972, good precision (RSD = 1.54 ± 0.11%), and recovery at three different levels of concentration was found between 98.33% and 103.47%. Usefulness of the method was demonstrated by positive results obtained during determination of bacitracin concentration in bulk drug. | pl |
| dc.affiliation | Wydział Farmaceutyczny : Zakład Chemii Nieorganicznej | pl |
| dc.affiliation | Wydział Farmaceutyczny : Zakład Chemii Analitycznej | pl |
| dc.contributor.author | Krzek, Jan - 130468 | pl |
| dc.contributor.author | Piotrowska, Joanna - 184976 | pl |
| dc.date.accession | 2020-07-28 | pl |
| dc.date.accessioned | 2020-07-28T12:25:29Z | |
| dc.date.available | 2020-07-28T12:25:29Z | |
| dc.date.issued | 2011 | pl |
| dc.date.openaccess | 0 | |
| dc.description.accesstime | w momencie opublikowania | |
| dc.description.additional | Bibliogr. s. 858 | pl |
| dc.description.number | 6 | pl |
| dc.description.physical | 853-858 | pl |
| dc.description.publication | 0,31 | pl |
| dc.description.version | ostateczna wersja wydawcy | |
| dc.description.volume | 68 | pl |
| dc.identifier.eissn | 2353-5288 | pl |
| dc.identifier.issn | 0001-6837 | pl |
| dc.identifier.project | ROD UJ / OP | pl |
| dc.identifier.uri | https://ruj.uj.edu.pl/xmlui/handle/item/242950 | |
| dc.identifier.weblink | https://www.ptfarm.pl/wydawnictwa/czasopisma/acta-poloniae-pharmaceutica/110/-/13706 | pl |
| dc.language | eng | pl |
| dc.language.container | eng | pl |
| dc.rights | Udzielam licencji. Uznanie autorstwa - Użycie niekomercyjne 4.0 Międzynarodowa | * |
| dc.rights.licence | CC-BY-NC | |
| dc.rights.uri | http://creativecommons.org/licenses/by-nc/4.0/legalcode.pl | * |
| dc.share.type | otwarte czasopismo | |
| dc.subject.en | bacitracin | pl |
| dc.subject.en | dabsyl chloride | pl |
| dc.subject.en | VIS spectrophotometry | pl |
| dc.subtype | Article | pl |
| dc.title | Spectrophotometric determination of bacitracin in bulk drug as dabsyl derivative in a range of visible light | pl |
| dc.title.journal | Acta Poloniae Pharmaceutica. Drug Research | pl |
| dc.type | JournalArticle | pl |
| dspace.entity.type | Publication |
dc.abstract.enpl
A fast spectrophotometric method has been developed for bacitracin identification and determination after condensation reaction with dabsyl chloride. In addition, determination of dye stability of sulfonamide derivative and identification of the molar ratio of reagents was done at various time-points. The developed method has a good linearity with very broad spectrum, correlation coefficient of r = 0.9972, good precision (RSD = 1.54 ± 0.11%), and recovery at three different levels of concentration was found between 98.33% and 103.47%. Usefulness of the method was demonstrated by positive results obtained during determination of bacitracin concentration in bulk drug. dc.affiliationpl
Wydział Farmaceutyczny : Zakład Chemii Nieorganicznej dc.affiliationpl
Wydział Farmaceutyczny : Zakład Chemii Analitycznej dc.contributor.authorpl
Krzek, Jan - 130468 dc.contributor.authorpl
Piotrowska, Joanna - 184976 dc.date.accessionpl
2020-07-28 dc.date.accessioned
2020-07-28T12:25:29Z dc.date.available
2020-07-28T12:25:29Z dc.date.issuedpl
2011 dc.date.openaccess
0 dc.description.accesstime
w momencie opublikowania dc.description.additionalpl
Bibliogr. s. 858 dc.description.numberpl
6 dc.description.physicalpl
853-858 dc.description.publicationpl
0,31 dc.description.version
ostateczna wersja wydawcy dc.description.volumepl
68 dc.identifier.eissnpl
2353-5288 dc.identifier.issnpl
0001-6837 dc.identifier.projectpl
ROD UJ / OP dc.identifier.uri
https://ruj.uj.edu.pl/xmlui/handle/item/242950 dc.identifier.weblinkpl
https://www.ptfarm.pl/wydawnictwa/czasopisma/acta-poloniae-pharmaceutica/110/-/13706 dc.languagepl
eng dc.language.containerpl
eng dc.rights*
Udzielam licencji. Uznanie autorstwa - Użycie niekomercyjne 4.0 Międzynarodowa dc.rights.licence
CC-BY-NC dc.rights.uri*
http://creativecommons.org/licenses/by-nc/4.0/legalcode.pl dc.share.type
otwarte czasopismo dc.subject.enpl
bacitracin dc.subject.enpl
dabsyl chloride dc.subject.enpl
VIS spectrophotometry dc.subtypepl
Article dc.titlepl
Spectrophotometric determination of bacitracin in bulk drug as dabsyl derivative in a range of visible light dc.title.journalpl
Acta Poloniae Pharmaceutica. Drug Research dc.typepl
JournalArticle dspace.entity.type
Publication Affiliations
No affiliation
Krzek, Jan
Piotrowska, Joanna
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