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Structural and textural evolution of zirconia nanocrystals induced by thermal treatment
2008
journal article
article
Journal
Materials Science Poland
Author
Adamski Andrzej
Jakubus P.
Sojka Zbigniew
Volume
26
Number
2
Pages
373-380
ISSN
2083-1331
eISSN
2083-134X
Keywords in English
nanostructured ZrO2
polymorphism
thermal evolution
grain size
Access date
2020-12-03
Remarks
Bibliogr. s. 380.
Language
English
Journal language
English
Abstract in English
Nanometric tetragonal and monoclinic zirconia was synthesized from zirconyl chloride by the modified forced hydrolysis method. Phase transitions and morphological changes accompanying zirconia calcination in the temperaure range 600–1000 °C were studied by XRD, HR-TEM techniques and N2-porosimetry. Ageing of the amorphous hydrous zirconia at 100 °C for 48 h in the mother solution and its subsequent calcination at 600 °C for 6 h strongly favoured formation of single-phase tetragonal ZrO2 of the thermal stability enhanced by 250 °C. Influence of the calcination temperature on phase composition, grain size, grain boundaries and pore structure of the resultant ZrO2 material was analyzed.
Affiliation
Wydział Chemii : Zakład Chemii NieorganicznejWydział Chemii : Zakład Chemii Środowiska
| dc.abstract.en | Nanometric tetragonal and monoclinic zirconia was synthesized from zirconyl chloride by the modified forced hydrolysis method. Phase transitions and morphological changes accompanying zirconia calcination in the temperaure range 600–1000 °C were studied by XRD, HR-TEM techniques and N2-porosimetry. Ageing of the amorphous hydrous zirconia at 100 °C for 48 h in the mother solution and its subsequent calcination at 600 °C for 6 h strongly favoured formation of single-phase tetragonal ZrO2 of the thermal stability enhanced by 250 °C. Influence of the calcination temperature on phase composition, grain size, grain boundaries and pore structure of the resultant ZrO2 material was analyzed. | pl |
| dc.affiliation | Wydział Chemii : Zakład Chemii Nieorganicznej | pl |
| dc.affiliation | Wydział Chemii : Zakład Chemii Środowiska | pl |
| dc.contributor.author | Adamski, Andrzej - 127117 | pl |
| dc.contributor.author | Jakubus, P. | pl |
| dc.contributor.author | Sojka, Zbigniew - 131982 | pl |
| dc.date.accession | 2020-12-03 | pl |
| dc.date.accessioned | 2020-12-03T14:11:12Z | |
| dc.date.available | 2020-12-03T14:11:12Z | |
| dc.date.issued | 2008 | pl |
| dc.date.openaccess | 0 | |
| dc.description.accesstime | w momencie opublikowania | |
| dc.description.additional | Bibliogr. s. 380. | pl |
| dc.description.number | 2 | pl |
| dc.description.physical | 373-380 | pl |
| dc.description.version | ostateczna wersja wydawcy | |
| dc.description.volume | 26 | pl |
| dc.identifier.eissn | 2083-134X | pl |
| dc.identifier.issn | 2083-1331 | pl |
| dc.identifier.project | ROD UJ / OP | pl |
| dc.identifier.uri | https://ruj.uj.edu.pl/xmlui/handle/item/258082 | |
| dc.identifier.weblink | http://www.materialsscience.pwr.wroc.pl/bi/vol26no2/articles/ms_2007_46PRO09.pdf | pl |
| dc.language | eng | pl |
| dc.language.container | eng | pl |
| dc.rights | Udzielam licencji. Uznanie autorstwa - Użycie niekomercyjne - Bez utworów zależnych 3.0 | * |
| dc.rights.licence | CC-BY-NC-ND | |
| dc.rights.uri | http://creativecommons.org/licenses/by-nc-nd/3.0/legalcode | * |
| dc.share.type | otwarte czasopismo | |
| dc.source.integrator | false | |
| dc.subject.en | nanostructured ZrO2 | pl |
| dc.subject.en | polymorphism | pl |
| dc.subject.en | thermal evolution | pl |
| dc.subject.en | grain size | pl |
| dc.subtype | Article | pl |
| dc.title | Structural and textural evolution of zirconia nanocrystals induced by thermal treatment | pl |
| dc.title.journal | Materials Science Poland | pl |
| dc.type | JournalArticle | pl |
| dspace.entity.type | Publication |
dc.abstract.enpl
Nanometric tetragonal and monoclinic zirconia was synthesized from zirconyl chloride by the modified forced hydrolysis method. Phase transitions and morphological changes accompanying zirconia
calcination in the temperaure range 600–1000 °C were studied by XRD, HR-TEM techniques and
N2-porosimetry. Ageing of the amorphous hydrous zirconia at 100 °C for 48 h in the mother solution and
its subsequent calcination at 600 °C for 6 h strongly favoured formation of single-phase tetragonal ZrO2
of the thermal stability enhanced by 250 °C. Influence of the calcination temperature on phase composition, grain size, grain boundaries and pore structure of the resultant ZrO2 material was analyzed. dc.affiliationpl
Wydział Chemii : Zakład Chemii Nieorganicznej dc.affiliationpl
Wydział Chemii : Zakład Chemii Środowiska dc.contributor.authorpl
Adamski, Andrzej - 127117 dc.contributor.authorpl
Jakubus, P. dc.contributor.authorpl
Sojka, Zbigniew - 131982 dc.date.accessionpl
2020-12-03 dc.date.accessioned
2020-12-03T14:11:12Z dc.date.available
2020-12-03T14:11:12Z dc.date.issuedpl
2008 dc.date.openaccess
0 dc.description.accesstime
w momencie opublikowania dc.description.additionalpl
Bibliogr. s. 380. dc.description.numberpl
2 dc.description.physicalpl
373-380 dc.description.version
ostateczna wersja wydawcy dc.description.volumepl
26 dc.identifier.eissnpl
2083-134X dc.identifier.issnpl
2083-1331 dc.identifier.projectpl
ROD UJ / OP dc.identifier.uri
https://ruj.uj.edu.pl/xmlui/handle/item/258082 dc.identifier.weblinkpl
http://www.materialsscience.pwr.wroc.pl/bi/vol26no2/articles/ms_2007_46PRO09.pdf dc.languagepl
eng dc.language.containerpl
eng dc.rights*
Udzielam licencji. Uznanie autorstwa - Użycie niekomercyjne - Bez utworów zależnych 3.0 dc.rights.licence
CC-BY-NC-ND dc.rights.uri*
http://creativecommons.org/licenses/by-nc-nd/3.0/legalcode dc.share.type
otwarte czasopismo dc.source.integrator
false dc.subject.enpl
nanostructured ZrO2 dc.subject.enpl
polymorphism dc.subject.enpl
thermal evolution dc.subject.enpl
grain size dc.subtypepl
Article dc.titlepl
Structural and textural evolution of zirconia nanocrystals induced by thermal treatment dc.title.journalpl
Materials Science Poland dc.typepl
JournalArticle dspace.entity.type
Publication Affiliations
No affiliation
Adamski, Andrzej
Jakubus, P.
Sojka, Zbigniew
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