X-ray spectroscopy station for sample characterization at ELI Beamlines

2023
journal article
article
3
dc.abstract.enX-ray spectroscopy is a demanded tool across multiple user communities. Here we report on a new station for X-ray emission spectroscopy at the Extreme Light Infrastructure Beamlines Facility. The instrument utilizes the von Hamos geometry and works with a number of different sample types, notably including liquid systems. We demonstrate a simple and reliable method for source position control using two cameras. This approach addresses energy calibration dependence on sample position, which is a characteristic source of measurement uncertainty for wavelength dispersive spectrometers in XES arrangement. We also present a straightforward procedure for energy calibration of liquid and powder samples to a thin film reference. The developed instrumentation enabled us to perform the first experimental determination of the Kα lines of liquidized K3Fe(CN)6 as well as powdered and liquidized FeNH4(SO4)2. Finally, we report on proof-of-principle use of a colliding jet liquid sample delivery system in an XES experiment.
dc.affiliationPion Prorektora ds. badań naukowych : Narodowe Centrum Promieniowania Synchrotronowego SOLARIS
dc.contributor.authorZymaková, A.
dc.contributor.authorPrecek, M.
dc.contributor.authorPicchiotti, A.
dc.contributor.authorBłachucki, W.
dc.contributor.authorZymak, I
dc.contributor.authorSzlachetko, Jakub - 432308
dc.contributor.authorVankó, G.
dc.contributor.authorZ. Németh
dc.contributor.authorSá, J.
dc.contributor.authorT. Wiste
dc.contributor.authorAndreasson, J.
dc.date.accessioned2024-05-17T12:34:58Z
dc.date.available2024-05-17T12:34:58Z
dc.date.issued2023
dc.date.openaccess0
dc.description.accesstimew momencie opublikowania
dc.description.versionostateczna wersja wydawcy
dc.description.volume13
dc.identifier.articleid17258
dc.identifier.doi10.1038/s41598-023-43924-y
dc.identifier.issn2045-2322
dc.identifier.urihttps://ruj.uj.edu.pl/handle/item/340550
dc.languageeng
dc.language.containereng
dc.rightsUdzielam licencji. Uznanie autorstwa 4.0 Międzynarodowa
dc.rights.licenceCC-BY
dc.rights.urihttp://creativecommons.org/licenses/by/4.0/legalcode.pl
dc.share.typeotwarte czasopismo
dc.source.integratorfalse
dc.subtypeArticle
dc.titleX-ray spectroscopy station for sample characterization at ELI Beamlines
dc.title.journalScientific Reports
dc.typeJournalArticle
dspace.entity.typePublicationen
dc.abstract.en
X-ray spectroscopy is a demanded tool across multiple user communities. Here we report on a new station for X-ray emission spectroscopy at the Extreme Light Infrastructure Beamlines Facility. The instrument utilizes the von Hamos geometry and works with a number of different sample types, notably including liquid systems. We demonstrate a simple and reliable method for source position control using two cameras. This approach addresses energy calibration dependence on sample position, which is a characteristic source of measurement uncertainty for wavelength dispersive spectrometers in XES arrangement. We also present a straightforward procedure for energy calibration of liquid and powder samples to a thin film reference. The developed instrumentation enabled us to perform the first experimental determination of the Kα lines of liquidized K3Fe(CN)6 as well as powdered and liquidized FeNH4(SO4)2. Finally, we report on proof-of-principle use of a colliding jet liquid sample delivery system in an XES experiment.
dc.affiliation
Pion Prorektora ds. badań naukowych : Narodowe Centrum Promieniowania Synchrotronowego SOLARIS
dc.contributor.author
Zymaková, A.
dc.contributor.author
Precek, M.
dc.contributor.author
Picchiotti, A.
dc.contributor.author
Błachucki, W.
dc.contributor.author
Zymak, I
dc.contributor.author
Szlachetko, Jakub - 432308
dc.contributor.author
Vankó, G.
dc.contributor.author
Z. Németh
dc.contributor.author
Sá, J.
dc.contributor.author
T. Wiste
dc.contributor.author
Andreasson, J.
dc.date.accessioned
2024-05-17T12:34:58Z
dc.date.available
2024-05-17T12:34:58Z
dc.date.issued
2023
dc.date.openaccess
0
dc.description.accesstime
w momencie opublikowania
dc.description.version
ostateczna wersja wydawcy
dc.description.volume
13
dc.identifier.articleid
17258
dc.identifier.doi
10.1038/s41598-023-43924-y
dc.identifier.issn
2045-2322
dc.identifier.uri
https://ruj.uj.edu.pl/handle/item/340550
dc.language
eng
dc.language.container
eng
dc.rights
Udzielam licencji. Uznanie autorstwa 4.0 Międzynarodowa
dc.rights.licence
CC-BY
dc.rights.uri
http://creativecommons.org/licenses/by/4.0/legalcode.pl
dc.share.type
otwarte czasopismo
dc.source.integrator
false
dc.subtype
Article
dc.title
X-ray spectroscopy station for sample characterization at ELI Beamlines
dc.title.journal
Scientific Reports
dc.type
JournalArticle
dspace.entity.typeen
Publication
Affiliations

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