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Salen impregnated silica gel as a new sorbent for on-line preconcentration of cadmium(II)

Salen impregnated silica gel as a new sorbent for ...

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dc.contributor.author Gawin, Marta [SAP14000661] pl
dc.contributor.author Bryłka, Martyna pl
dc.contributor.author Mrowiec, Halina [SAP12006408] pl
dc.contributor.author Telk, Anna [SAP14000589] pl
dc.contributor.author Trzewik, Bartosz [SAP11018750] pl
dc.contributor.author Walas, Stanisław [SAP11008764] pl
dc.date.accessioned 2015-08-26T10:52:02Z
dc.date.available 2015-08-26T10:52:02Z
dc.date.issued 2011 pl
dc.identifier.issn 0306-7319 pl
dc.identifier.uri http://ruj.uj.edu.pl/xmlui/handle/item/15052
dc.language eng pl
dc.title Salen impregnated silica gel as a new sorbent for on-line preconcentration of cadmium(II) pl
dc.type JournalArticle pl
dc.description.physical 484-492 pl
dc.description.additional Na publikacji autorka Telk Anna podpisana jako Tobiasz Anna. pl
dc.abstract.en A new sorbent – salen impregnated silica gel – was prepared and characterised for application as a minicolumn packing for flow-injection on-line preconcentration of cadmium(II). The system was coupled with flame atomic absorption spectrometer (FI-FAAS). The optimal pH for Cd(II) sorption was in the range of 7.4–8.8 and nitric acid (1%, v/v) was efficient as eluent. Sorption was most effective within the sample flow rate up to 7 mL min−1. Sorption capacity of the sorbent found in a batch procedure was 26.3 µmol g−1 (2.95 mg g−1). Enrichment factor (EF) and limit of detection (LOD) obtained for 120-second loading time were 113 and 0.26 µg L−1, respectively. The sorbent stability in the working conditions was proved for at least 100 preconcentration cycles. The evaluated method was applied to Cd(II) determination in various water samples. pl
dc.description.volume 91 pl
dc.description.number 5 pl
dc.description.points 20 pl
dc.identifier.doi 10.1080/03067310903229935 pl
dc.identifier.eissn 1029-0397 pl
dc.identifier.eissn 1026-7468 pl
dc.title.journal International Journal of Environmental Analytical Chemistry pl
dc.language.container eng pl
dc.affiliation Wydział Chemii : Zakład Chemii Analitycznej pl
dc.affiliation Wydział Chemii : Zakład Chemii Organicznej pl
dc.subtype Article pl
.pointsMNiSW [2011 A]: 20


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