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Visualization of amphetamine and its analogues in TLC

2007
journal article
article
Journal
Acta Chimica Slovenica
Author
Zakrzewska Agnieszka

Parczewski Andrzej

Kaźmierczak D.

Ciesielski W.

Kochana Jolanta
Volume
54
Number
1
Pages
106-109
ISSN
1318-0207
eISSN
1580-3155
Keywords in English

TLC

iodine azide reaction

visualization of amphetamines

URL
http://acta-arhiv.chem-soc.si/54/54-1-106.pdf
Access date
2020-12-08
Remarks

Bibliogr. s. 109.

Language
English
Journal language
English
Abstract in English

Derivatisation followed by iodine azide reaction was employed for detection of amphetamines and its analogues in TLC. The derivatisation reaction with phenyl isothiocyanate took place directly on the TLC plate before the developing step. Afterwards, the plate was sprayed with a mixture of sodium azide and starch solution and then exposed to iodine vapour. The obtained limits of detection were compared with other commonly visualization techniques: UV, iodine vapour, Marquis and Simon’s reagents, ninhydrin, Fast Black K.

Affiliation
Wydział Chemii : Zakład Chemii Analitycznej
dc.abstract.enDerivatisation followed by iodine azide reaction was employed for detection of amphetamines and its analogues in TLC. The derivatisation reaction with phenyl isothiocyanate took place directly on the TLC plate before the developing step. Afterwards, the plate was sprayed with a mixture of sodium azide and starch solution and then exposed to iodine vapour. The obtained limits of detection were compared with other commonly visualization techniques: UV, iodine vapour, Marquis and Simon’s reagents, ninhydrin, Fast Black K.pl
dc.affiliationWydział Chemii : Zakład Chemii Analitycznejpl
dc.contributor.authorZakrzewska, Agnieszka - 198214 pl
dc.contributor.authorParczewski, Andrzej - 131278 pl
dc.contributor.authorKaźmierczak, D.pl
dc.contributor.authorCiesielski, W.pl
dc.contributor.authorKochana, Jolanta - 128954 pl
dc.date.accession2020-12-08pl
dc.date.accessioned2020-12-08T21:45:28Z
dc.date.available2020-12-08T21:45:28Z
dc.date.issued2007pl
dc.date.openaccess0
dc.description.accesstimew momencie opublikowania
dc.description.additionalBibliogr. s. 109.pl
dc.description.number1pl
dc.description.physical106-109pl
dc.description.versionostateczna wersja wydawcy
dc.description.volume54pl
dc.identifier.eissn1580-3155pl
dc.identifier.issn1318-0207pl
dc.identifier.projectROD UJ / OPpl
dc.identifier.urihttps://ruj.uj.edu.pl/xmlui/handle/item/258472
dc.identifier.weblinkhttp://acta-arhiv.chem-soc.si/54/54-1-106.pdfpl
dc.languageengpl
dc.language.containerengpl
dc.rightsUdzielam licencji. Uznanie autorstwa 4.0 Międzynarodowa*
dc.rights.licenceCC-BY
dc.rights.urihttp://creativecommons.org/licenses/by/4.0/legalcode.pl*
dc.share.typeotwarte czasopismo
dc.subject.enTLCpl
dc.subject.eniodine azide reactionpl
dc.subject.envisualization of amphetaminespl
dc.subtypeArticlepl
dc.titleVisualization of amphetamine and its analogues in TLCpl
dc.title.journalActa Chimica Slovenicapl
dc.typeJournalArticlepl
dspace.entity.typePublication
dc.abstract.enpl
Derivatisation followed by iodine azide reaction was employed for detection of amphetamines and its analogues in TLC. The derivatisation reaction with phenyl isothiocyanate took place directly on the TLC plate before the developing step. Afterwards, the plate was sprayed with a mixture of sodium azide and starch solution and then exposed to iodine vapour. The obtained limits of detection were compared with other commonly visualization techniques: UV, iodine vapour, Marquis and Simon’s reagents, ninhydrin, Fast Black K.
dc.affiliationpl
Wydział Chemii : Zakład Chemii Analitycznej
dc.contributor.authorpl
Zakrzewska, Agnieszka - 198214
dc.contributor.authorpl
Parczewski, Andrzej - 131278
dc.contributor.authorpl
Kaźmierczak, D.
dc.contributor.authorpl
Ciesielski, W.
dc.contributor.authorpl
Kochana, Jolanta - 128954
dc.date.accessionpl
2020-12-08
dc.date.accessioned
2020-12-08T21:45:28Z
dc.date.available
2020-12-08T21:45:28Z
dc.date.issuedpl
2007
dc.date.openaccess
0
dc.description.accesstime
w momencie opublikowania
dc.description.additionalpl
Bibliogr. s. 109.
dc.description.numberpl
1
dc.description.physicalpl
106-109
dc.description.version
ostateczna wersja wydawcy
dc.description.volumepl
54
dc.identifier.eissnpl
1580-3155
dc.identifier.issnpl
1318-0207
dc.identifier.projectpl
ROD UJ / OP
dc.identifier.uri
https://ruj.uj.edu.pl/xmlui/handle/item/258472
dc.identifier.weblinkpl
http://acta-arhiv.chem-soc.si/54/54-1-106.pdf
dc.languagepl
eng
dc.language.containerpl
eng
dc.rights*
Udzielam licencji. Uznanie autorstwa 4.0 Międzynarodowa
dc.rights.licence
CC-BY
dc.rights.uri*
http://creativecommons.org/licenses/by/4.0/legalcode.pl
dc.share.type
otwarte czasopismo
dc.subject.enpl
TLC
dc.subject.enpl
iodine azide reaction
dc.subject.enpl
visualization of amphetamines
dc.subtypepl
Article
dc.titlepl
Visualization of amphetamine and its analogues in TLC
dc.title.journalpl
Acta Chimica Slovenica
dc.typepl
JournalArticle
dspace.entity.type
Publication
Affiliations
No affiliation
Zakrzewska, Agnieszka
Parczewski, Andrzej
Kaźmierczak, D.
Ciesielski, W.
Kochana, Jolanta

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