Powder diffraction and synchrotron radiation, a powerful tool in the investigation of new compounds : and

2015
journal article
article
dc.abstract.enUsing synchrotron powder diffraction data, two new complexes of CdBr2 with 3-fluoroaniline and 4-fluoroaniline were fully characterised with regard to their structure. Their crystal structures were solved and refined by means of powder diffraction techniques. The investigated materials belong to the group of hybrid inorganic–organic coordination polymers. The structures of both compounds are created by the same type, infinite chains formed by CdBr4N2 octahedra. Each cadmium cation is surrounded by four Br− anions, and two N atoms from two fluoroaniline molecules. The obtained structural data enable us to investigate the influence of the position of the F atom in the aniline ring on the crystal structure, as well as to interpret its thermal stability.pl
dc.affiliationWydział Chemii : Zakład Krystalochemii i Krystalofizykipl
dc.contributor.authorGrzesiak-Nowak, Marta - 107639 pl
dc.contributor.authorŁasocha, Wiesław - 130062 pl
dc.contributor.authorAppleby, Grahampl
dc.date.accessioned2015-12-29T07:20:55Z
dc.date.available2015-12-29T07:20:55Z
dc.date.issued2015pl
dc.description.additionalŁasocha W. afiliuje z Wydziału Chemii UJ; Grzesiak-Nowak nie afiliuje.pl
dc.description.admin[AU] Grzesiak-Nowak, Marta [SAP14001272]pl
dc.description.number5pl
dc.description.physical398-403pl
dc.description.volume44pl
dc.identifier.doi10.1002/xrs.2647pl
dc.identifier.eissn1097-4539pl
dc.identifier.issn0049-8246pl
dc.identifier.urihttp://ruj.uj.edu.pl/xmlui/handle/item/18701
dc.languageengpl
dc.language.containerengpl
dc.rights.licencebez licencji
dc.subtypeArticlepl
dc.titlePowder diffraction and synchrotron radiation, a powerful tool in the investigation of new compounds : $CdBr_2(3-fluoroaniline)_2$ and $CdBr_2(4-fluoroaniline)_2$pl
dc.title.journalX-Ray Spectrometrypl
dc.title.volumeSpecial Issue: 10th Jubilee national symposium of synchrotron radiation users, 9–11 September 2013, Stalowa Wola, Polandpl
dc.typeJournalArticlepl
dspace.entity.typePublication
dc.abstract.enpl
Using synchrotron powder diffraction data, two new complexes of CdBr2 with 3-fluoroaniline and 4-fluoroaniline were fully characterised with regard to their structure. Their crystal structures were solved and refined by means of powder diffraction techniques. The investigated materials belong to the group of hybrid inorganic–organic coordination polymers. The structures of both compounds are created by the same type, infinite chains formed by CdBr4N2 octahedra. Each cadmium cation is surrounded by four Br− anions, and two N atoms from two fluoroaniline molecules. The obtained structural data enable us to investigate the influence of the position of the F atom in the aniline ring on the crystal structure, as well as to interpret its thermal stability.
dc.affiliationpl
Wydział Chemii : Zakład Krystalochemii i Krystalofizyki
dc.contributor.authorpl
Grzesiak-Nowak, Marta - 107639
dc.contributor.authorpl
Łasocha, Wiesław - 130062
dc.contributor.authorpl
Appleby, Graham
dc.date.accessioned
2015-12-29T07:20:55Z
dc.date.available
2015-12-29T07:20:55Z
dc.date.issuedpl
2015
dc.description.additionalpl
Łasocha W. afiliuje z Wydziału Chemii UJ; Grzesiak-Nowak nie afiliuje.
dc.description.adminpl
[AU] Grzesiak-Nowak, Marta [SAP14001272]
dc.description.numberpl
5
dc.description.physicalpl
398-403
dc.description.volumepl
44
dc.identifier.doipl
10.1002/xrs.2647
dc.identifier.eissnpl
1097-4539
dc.identifier.issnpl
0049-8246
dc.identifier.uri
http://ruj.uj.edu.pl/xmlui/handle/item/18701
dc.languagepl
eng
dc.language.containerpl
eng
dc.rights.licence
bez licencji
dc.subtypepl
Article
dc.titlepl
Powder diffraction and synchrotron radiation, a powerful tool in the investigation of new compounds : $CdBr_2(3-fluoroaniline)_2$ and $CdBr_2(4-fluoroaniline)_2$
dc.title.journalpl
X-Ray Spectrometry
dc.title.volumepl
Special Issue: 10th Jubilee national symposium of synchrotron radiation users, 9–11 September 2013, Stalowa Wola, Poland
dc.typepl
JournalArticle
dspace.entity.type
Publication

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